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Figure 2

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The nanocrystalline domains in NC-NbSe2 film. (A, B) Large-scale and (C) zoom-in high-resolution TEM images, and (inset in (C)) Fourier transform pattern of crystalline NbSe2 (C-NbSe2) film grown on a sapphire substrate as comparison. (D) A large-scale TEM image showing the uniformity of as-grown NC-NbSe2 film on SiO2/Si substrate. (E) The EDS spectrum and (F) SAED pattern of as-grown NC-NbSe2 film. Notably, the Cu Kα signal in panel (E) sources from the TEM grid. (G) A representative high-resolution TEM image with (H) false color and crystalline orientation superimposed to highlight nano-domain in NC-NbSe2 film. (I) A representative grain boundary between nano-domain in NC-NbSe2 film.

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